Electrospun micro and nanofibers produced via electrospinning method were used for the sound absorption purposes. Polymers were initially dissolved in dimethyleformamide (DMF) or ethanol with a ratio of 80:20 and electrospun at 20 kV, 20 cm separation distance and 3 ml/hrs pump speed. The two-microphone transfer function method of the B&K impedance tube was used to determine the acoustical properties of the manufactured nanofibers at various frequencies. The test results showed that the absorption coefficients of nanofibers (~500 nm) drastically increased. The reason behind this phenomenon may be attributed to the higher surface area of nanofibers and their interactions with more sound waves/air molecules. This result may open up new possibilities for the sound absorption problems in many fields, such as aircrafts, other transportation vehicles and infrastructures.